基于紫外指纹图谱的公英青蓝合剂质量研究

doi:10.16431/j.cnki.1671-7236.2017.02.038

Abstract

Abstract:

To establish UV fingerprint method of measuring Gongyingqinglan mixture quality,UV fingerprints were got using ultraviolet spectrophotometer scanning ten Gongyingqinglan mixture,and the correlation coefficient method was used to calculate the similarity between Gongyingqinglan mixture sample fingerprints and contrasted fingerprint. The results showed that the UV fingerprint absorbance of samples that chlorogenic acid content conformed with the provisions were 0.165-0.265 Abs (317.00 nm),0.162-0.285 Abs (282.00 nm) and 0.137-0.240 Abs (259.00 nm),and the fingerprint similarity was above 0.910.While the UV fingerprint absorbance of samples that chlorogenic acid content was not in conformity with the provisions did not meet this condition of 0.165-0.265 Abs (317.00 nm),0.162-0.285 Abs (282.00 nm) and 0.137-0.240 Abs (259.00 nm) or the fingerprint similarity were below 0.910.This method could be used to control the quality of the Gongyingqinglan mixture.

Key words: Gongyingqinglan mixture; fingerprint; chlorogenic acid; quality standard

CLC Number:

R284

PAN Chun-hui, YANG Hong-yu, ZHANG Xuan, REN Yuan-qin, PENG Xiao-feng, YONG Ling, LIU Tao. Study on the UV Fingerprint of Gongyingqinglan Mixture[J]. , 2017, 44(2): 578-585.

References

[1] 董付哲.鸡非典型传染性法氏囊病的发病特征与防治措施[J].中国畜牧兽医文摘,2016,32(1):158.
[2] 袁汀,王美,张振秋.月矾中空栓高效液相特征图谱研究[J].辽宁中医药大学学报,2014,16(12):47-50.
[3] 丰加涛,金郁,王金成,等.基于定量指纹图谱技术的中药质量控制[J].色谱,2008,26(2):180-185.
[4] 张娅,王丽娜,高敏.中药指纹图谱的发展现状及其在质量控制中的应用[J].云南中医中药杂志,2010,31(11):69-71.
[5] Marie A,Fournier F,Tabet J C. Characterization of synthetic polymers by MALDI-TOF/MS:Investigation into new methods of sample target preparation and consequence on mass spectrum finger print[J]. Analytical Chemistry,2000,72(20):5106-5114.
[6] 李强,杜思邈,张忠亮,等.中药指纹图谱技术进展及未来发展方向展望[J].中草药,2013,44(22):3095-3104.
[7] 刘江,陈兴福,邹元锋. 基于中药指纹图谱多维信息的化学模式识别研究进展[J].中国中药杂志,2012,37(8):1081-1088.
[8] 陈林伟,秦昆明,徐雪松,等.中药指纹图谱数据库的研究现状及展望[J].中草药,2014,45(21):3041-3046.
[9] 冯仁丰.再说说精密度[J].检验医学,2014,29(8):787-793.
[10] 王润群,朱清根,彭建勇,等.紫外法测定红土壤中的硝态氮[J].现代农业科技,2013,(13):242-244.
[11] 杨海峰,李勇军,金礼琴,等.吡喹酮注射液的含量测定及稳定性研究[J].中国畜牧兽医,2015,42(11):3010-3015.
[12] 丁青龙,李莹.紫外分光光度法测定复方苦参素胶囊中绞股蓝总皂苷含量及稳定性研究[J].江苏药学与临床研究,2004,12(5):25-26.
[13] 孔迪,彭观良,杨建坤,等.紫外可见分光光度计主要技术指标及其检定方法[J].大学物理实验,2007,20(4):1-6.
[14] 刘涛,伍利华,黄英,等.基于光谱法的清脑复神液指纹图谱研究[J].中国测试,2016,42(2):63-66.
[15] 孙国祥,杨婷婷,车磊.UV-IR光谱指纹定量法鉴定六味地黄丸质量[J].中南药学,2010,8(10):766-771.
[16] 阿吉姑·阿布都热西提,楚刚辉,徐云玲,等. 紫外指纹图谱在维吾尔药玫瑰花口服液质量控制中的应用[J].中国现代中药,2011,13(10):33-35.
[17] Yu L,Xu C,Zhu C. Probing the n→π* photoisomerization mechanism of cis-azobenzene by multi-state ab initio on-the-fly trajectory dynamics simulation[J]. Physical Chemistry Chemical Physics,2015,17(27):17646-17660.
[18] Haghdani S,Davari N,Sandnes R,et al.Complex frequency-dependent polarizability through the °π°→π°* excitation energy of azobenzene molecules by a combined charge-transfer and point-dipole interaction mode[J].The Journal of Physical Chemistry A,2014,118(47):11282-11292.
[19] Hidalgo M,Rivelino R,Canuto S.Origin of the red shift for the lowest singlet n→ π*° charge-transfer absorption of p-nitroaniline in supercritical CO₂[J].Journal of Chemical Theory and Computation,2014,10(4):1154-1562.
[20] Singh S K,Das A.The n→π* interaction:A rapidly emerging non-covalent interaction[J].Physical Chemistry Chemical Physics,2015,17(15):9596-9612.
[21] Chen Y,Wang B,Lin S,et al. Activation of n→π* transitions in two-dimensional conjugated polymers for visible light photocatalysis[J].The Journal of Physical Chemistry C,2014,118(51):29981-29989.
[22] Ferro-Costas D,Francisco E,Pendás Á M,et al. Revisiting the carbonyl n→π* electronic excitation through topological eyes:Expanding,enriching and enhancing the chemical language using electron number distribution functions and domain averaged fermi holes[J].Physical Chemistry Chemical Physics,2015,17(39):26059-26071.
[23] 关洪月,李林,刘晓,等. 中药指纹图谱相似度计算方法探析[J].中国实验方剂学杂志,2011,17(18):282-287.
[24] 孙国祥,李闫飞,邵艳玲,等.中药紫外指纹图谱超信息特征数字化和定量化评价方法研究[J].中南药学,2013,11(4):293-298.
[25] Liu Y C,Sun G X,Luan J Y,et al. A comprehensive strategy to monitor quality consistency of Weibizhi tablets based on integrated MIR and UV spectroscopic fingerprints,a systematically quantified fingerprint method,antioxidant activities and UPLC-Q-TOF-MS chemical profiling[J].RSC Advances,2016,6(1):366-375.

Study on the UV Fingerprint of Gongyingqinglan Mixture

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments

[1]	GENG Xiang, LIU Xiwang, YANG Yajun, LI Jianyong. Study on Quality Standard and Pharmaceutical Equivalence of Eprinomectin Sustain-release Injections [J]. China Animal Husbandry and Veterinary Medicine, 2021, 48(3): 1054-1063.
[2]	CUI Yange, LI Jingshuai, LI Yinju, ZHANG Chunjie. Inhibitory Effect of Chlorogenic Acid on FAdV-4 and Its Effects on the Expression of Inflammatory Factors and Signal Molecules in Chicken Embryo Liver [J]. China Animal Husbandry and Veterinary Medicine, 2021, 48(12): 4718-4724.
[3]	YAO Shanshan, ZHANG Shilei, LIANG Cunjun, ZHANG Tie, WANG Chunguang. Analysis of Bacteriostatic and Drug Resistance Elimination Mechanisms of Chicken-derived Escherichia coli by Chlorogenic Acid Based on Transcriptome Technology [J]. China Animal Husbandry and Veterinary Medicine, 2020, 47(12): 4156-4165.
[4]	LI Haihua, CHEN Zhiqiang, CAI Xiaoli, FU Liyun, GUO Weibing, ZHANG Pengju. Establishment a Chinese Medicine Quality Standard of Qinhong Perfusate for the Treatment of Mastitis [J]. China Animal Husbandry and Veterinary Medicine, 2019, 46(12): 3775-3784.
[5]	DENG Ruihan, LIN Bailiang, YANG Liu, LU Yanrong, PENG Jianbo, WU Wenjian, YANG Lei, HAO Zhihui, YANG Shanzhong, HE Jiakang. Thin Layer Chromatography Identification and Content Determination of Zhongjiefeng Sanqing Granule [J]. China Animal Husbandry and Veterinary Medicine, 2019, 46(10): 3095-3105.
[6]	ZHUO Chunliu, SHI Yuxiang, GAO Wei, LIN Dongmei, WANG Fangfang, XU Meili. Research Progress on Chlorogenic Acid in Animal Production [J]. China Animal Husbandry and Veterinary Medicine, 2019, 46(10): 3131-3136.
[7]	ZHU Hong-mei, LIU Cui, ZHANG Qian, ZHENG Qiu-yan, JIA Yu-jie, LIU Tao. Study on Quality Standard of Ruxiankang Injection [J]. , 2017, 44(8): 2465-2474.
[8]	PAN Chun-hui, YANG Hong-yu, ZHANG Xuan, REN Yuan-qin, PENG Xiao-feng, LIU Tao. Research on the Promotion of Qingwenbaidu Powder Quality Standard [J]. , 2016, 43(12): 3170-3176.
[9]	REN Li-hua, XIN Rui-hua, CHENG Long，LUO Yong-jiang, WANG Gui-bo, LUO Chao-ying, XIE Jia-sheng, LI Jin-yu, ZHENG Ji-fang. Study on Quality Standard of Jin Gen Qin Lian Powder [J]. , 2014, 41(8): 169-172.
[10]	CHENG Long, XIN Rui-hua, LUO Yong-jiang, WANG Gui-bo, LUO Chao-ying,XIE Jia-sheng,LI Jin-yu, ZHENG Ji-fang. Study on Quality Standard of Zhike Pingchuan Granules [J]. , 2014, 41(1): 141-145.
[11]	KANG Lian-lian, LIU-Qun, JIANG Ping-kang, YANG Song-pei, JI Li-li, LU Ya-yi, TANG Di. Preliminary Study on Quality Standard of Chinese Herbal Compound of Extract [J]. , 2013, (5): 218-221.
[12]	WANG Xue-hong;LIU Yu;GUO Wen-zhu;HAO Bao-cheng;ZHENG Hong-xing;LIANG Jian-ping. The Study on the Quality Standard of Pyroline [J]. , 2011, 38(9): 218-220.
[13]	LAN Xiao-yan;ZHANG Xue-jun. Studying on Quantitative Determination of Chlorogenic Acid in Eucommia Leaves [J]. , 2010, 37(4): 53-55.
[14]	LUO Jia-jie;LI Li-li;ZHANG Bin. T-RFLP Analysis Technique and its Application on Analyzing Microbial Community Structure [J]. , 2009, 36(7): 75-78.
[15]	WANG Xuebing;WEI Zhanyong;CUI Baoan;LI Changlei;XU Duanhong;CHEN Hongying. Extraction of Chlorogenic Acid from Chinese Herbal Medicine and its Antiviral Effect on Porcine Parvovirus in Vitro [J]. , 2008, 1(12): 123-125.