›› 2013, Vol. 40 ›› Issue (S1): 34-36.

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Microwave Digestion and Graphite Furnace Atomic Absorption Spectrometric Method for the Determination of Lead in Milk

PANG Xue-liang1, ZHENG Bai-qin1, LI Ai-jun1, DONG Li-xue1, GE Huai-li1, QI Biao2, ZHANG Jian-min1, ZHANG Xin1   

  1. 1. The Livestock and Aquatic Products Quality Inspection & Test Center(Tangshan), Tangshan 063000, China;
    2. The Central Agricultural Broadcasting and Television School of Tangshan Branch, Tangshan 063000, China
  • Received:2013-08-18 Online:2013-09-30 Published:2013-11-29

Abstract: A microwave digestion method was used in treatment of milk samples to determine lead conten. This method has the advantages of simple operation, less error. The lead in treatment solution was detected by atomic absorption spectrometry. The linear range of standardcurve was 0 to 40 ng/mL and the correlation coefficient was 0.9998. The recovery rates in milk lead were 90% to 95%. This method is not only exact and less error but also improving the detection efficiency.

Key words: microwave digestion; atomic absorption spectrometry; milk; lead

CLC Number: