麻疯树籽提油工艺优化及籽粕中粗蛋白质含量分析

doi:10.16431/j.cnki.1671-7236.2017.10.017

Abstract

Abstract:

The test was aimed to optimize the oil extraction process from Jatropha curcas seed and analyzed the crude protein content in meal.Jatropha curcas seeds were selected as the experimental material,and the effects of solid to liquid ratio,temperature and extraction time on the oil extraction rate and crude protein content of meal were investigated and optimized. The results of single factor test showed that when the solid to liquid ratio was 1:18,the temperature was 40℃ and extraction time was 30 min,the oil extraction rate was highest which was the 38.22%,32.21% and 34.13%,respectively. The variance analysis results showed that the order of factors that affected the oil extraction rate were temperature > solid to liquid ratio > extraction time. The effects of temperature and solid to liquid ratio were extremely significant (P < 0.01).The extraction time did not have a significant effect on oil extraction rate (P > 0.05).The order of factors that affected the crude protein content in seed meal were temperature > extraction time > solid to liquid ratio. The effect of temperature was extremely significant (P < 0.01) and that of the extraction time was significant (P < 0.05). The results of orthogonal experiment showed that the optimal extraction conditions was A₃B₃C₃ of which the solid to liquid ratio was 1:22,temperature was 50℃ and extraction time was 50 min. The oil extraction rate was 39.41%,and the crude protein was 24.13% under this condition. This study provided the theoretical basis for the development and application of Jatropha curcas seed.

Key words: Jatropha curcas seed; oil extraction process; oil extraction rate; Jatropha curcas meal; crude protein

CLC Number:

S816.4

XIE Kan, XIONG Chun-mei, FANG Li-yuan, JIANG Chan, LEI Fu-hong, OUYANG Wu-le, GUO Ai-wei. Optimization of Oil Extraction Process from Jatropha curcas Seed and the Analysis of Crude Protein Content in Meal[J]. , 2017, 44(10): 2951-2956.

References

[1] Rampadarath S,Puchooa D,Jeewon R.Jatropha curcas L. phytochemical,antimicrobial and larvicidal properties[J].Asian Pac J Trop Biomed,2016,6(10):858-865.
[2] Nithiyanantham S,Siddhuraju P,Francis G.Potential of Jatropha curcas as a biofuel,animal feed and health products[J].J Am Oil Chem Soc,2012,89(6):961-972.
[3] 刘泽铭,苏光荣,杨清.云南省麻疯树资源调查分析[J]. 林业科技开发,2008,22(1):37-40.
[4] Monteiro M V,Bevilaqua C M,Morais S M,et al.Anthelmintic activity of Jatropha curcas L. seeds on Haemonchus contortus[J].Vet Parasitol,2011,182(2-4):259-263.
[5] 孔令义,闵知大,史剑侠,等. 麻疯树根的化学成分研究[J].植物学报,1996,38(2):161-166.
[6] 李玲,李晓帆,吴慧星,等.麻疯树种子中抗氧化活性成分的研究[J].中草药,2010,41(12):1932-1936.
[7] Meher L C,Churamani C P,Arif M,et al.Jatropha curcas as a renewable source for biofuels:A review[J].Renew Sust Energ Rev,2013,26(10):397-407.
[8] Nzikou J M,Matos L,Mbemba F,et al.Characteristics and composition of Jatropha curcas oils,variety Congo-Brazzaville[J].Res J Appl Sci Eng Technol,2009,1(3):154-159.
[9] Foidl N,Foidl G,Sanchez M,et al. Jatropha curcas L. as a source for the production of biofuel in Nicaragua[J].Bioresour Technol,1996,58(1):77-82.
[10] King A J,He W,Cuevas J A,et al.Potential of Jatropha curcas as a source of renewable oil and animal feed[J].J Exp Bot,2009,60(10):2897-2905.
[11] Kumar V,Makkar H P S,Amselgruber W.Physiological,haematological and histopathological responses in common carp (Cyprinus carpio L.) fingerlings fed with differently detoxified Jatropha curcas kernel meal[J].Food Chem Toxicol,2010,48(8-9):2063-2072.
[12] Kumar V,Makkar H P S,Becker K.Detoxified Jatropha curcas kernel meal as a dietary protein source:Growth performance, nutrient utilization and digestive enzymes in common carp (Cyprinus carpio L.) fingerlings[J].Aquaculture Nutr,2011,17(3):313-326.
[13] Norfaezah A,Zainab H,Othman H.Comparative study between microwave assisted extraction and soxhlet extraction techniques for bio-oil extraction from Jatropha curcas[J].J Eng Sci and Technol,2015,8:9-16.
[14] 曾虹燕,方芳,苏杰龙,等.麻疯树籽油提取技术[J].江苏农业学报,2005,21(1):69-70.
[15] 张勤.生物统计学[M].第2版.北京:中国农业大学出版社,2008.
[16] Association of Official Analytical Chemists.Official methods of analysis[M].16th ed.Arlington:Association of official analytical chemists,1990.
[17] Subroto E,Manurung R,Heeres H J,et al.Optimization of mechanical oil extraction from Jatropha curcas L. kernel using response surface method[J].Ind Crops Prod,2015,63(12):294-302.
[18] 吕薇,蒋剑春,徐俊明.小桐子油脂提取工艺研究及脂肪酸组成分析[J].太阳能学报,2011,32(10):1500-1505.
[19] 易平,余启枝,屈文, 等.不同工艺提取麻疯树籽油及其杀灭血吸虫尾蚴效果[J].中国血吸虫病防治杂志,2014,26(2):187-191.
[20] Punsuvon V,Nokkaew R.Comparison of detoxification methods on phorbol esters in deoiled Jatropha curcas meal for animal feeds[J].J Chem Chem Eng,2013,7(6):533-538.
[21] 夏辉,陈燕,史宣明,等.95%乙醇浸出小桐子籽压榨饼工艺研究[J].中国油脂,2010,30(10):30-33.
[22] 万辉,夏辉,丁丹华,等.麻疯树籽蛋白提取工艺的研究[J].中国油脂,2010,35(3):28-31.
[23] 张靖楠,邱树毅.响应面法优化酶法提取麻疯树籽油工艺研究[J].粮食与油脂,2010,10:12-16.
[24] Sayyar S,Abidin Z Z,Yunus R,et al.Extraction of oil from Jatropha seeds optimization and kinetics[J].Am J Appl Sci,2009,6(7):1390-1395.
[25] Berchmans H,Hirata S.Biodiesel production from crude Jatropha curcas L. seed oil with a high content of free fatty acids[J].Bioresour Technol,2008,99(6):1716-1721.

Optimization of Oil Extraction Process from Jatropha curcas Seed and the Analysis of Crude Protein Content in Meal

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments

[1]	SUN Xiaoshan, LIN Dongmei, SHAO Yuxin, WANG Zheng, HUANG Jianguo. Study on the Changes of Crude Protein and Mineral Elements in Pigeon Milk at Different Ages [J]. China Animal Husbandry and Veterinary Medicine, 2022, 49(5): 1697-1706.
[2]	FAN Qiuli, RUAN Dong, JIANG Shouqun, CHENG Zhonggang, WANG Hanhua. Study on Dietary Crude Protein Requirement of Silky Fowl During 26 to 45 Days of Age [J]. China Animal Husbandry and Veterinary Medicine, 2022, 49(5): 1727-1737.
[3]	FAN Qiuli, JIANG Shouqun, WANG Hanhua, RUAN Dong, CHENG Zhonggang. Study on Dietary Crude Protein Requirement of Silky Fowl During 1 to 25 Days of Age [J]. China Animal Husbandry and Veterinary Medicine, 2022, 49(2): 501-509.
[4]	WEI Manhong, CHEN Yulin, YANG Yuxin. Technology Optimization of Soybean Meal Solid Fermentation by High-yielding Protease Yeast [J]. China Animal Husbandry and Veterinary Medicine, 2021, 48(7): 2431-2438.
[5]	ZHAO Xiaoyu, SHAERSHANBIEKE Abudilida, MA Chen, WU Yingping, WANG Junhua, LI Haiying. Effects of Dietary Crude Protein Level on Laying Raws,Reproductive Hormone Concentrations and Related Gene mRNA Expression in Reproductive Axis of Yili Geese [J]. China Animal Husbandry and Veterinary Medicine, 2020, 47(6): 1729-1738.
[6]	GONG Wenyang, LI Mo, NIU Yibing, DONG Xueyu, LI Yong, ZHANG Guixian, WANG Xiguo, GONG Yuanfang, SU Xin, YANG Liu, XING Guanzhong, FENG Minshan, LI Sufen. Effects of Dietary Protein and Ether Extract Levels on Nutrient Digestibility and Nitrogen Metabolism of Growing Raccoon Dogs [J]. China Animal Husbandry and Veterinary Medicine, 2020, 47(3): 763-770.
[7]	JIA Cunhui, QIAN Wenxi, TURSUNAY·Samat, GULPIYA·Abdukirem, AO Weiping. Effects of Feed Energy to Nitrogen Ratio on Rumen Fermentation in vitro of Tarim Red Deer [J]. , 2019, 46(6): 1619-1627.
[8]	ZHANG Ling, SUN Guobo, DUAN Xiujun, GU Wenjie, WANG Jian, QIN Haorong, GE Yuzhu, ZHANG Kai. Study on Metabolizable Energy, Crude Protein, Ca and Available P Contents in Black Muscovy Ducks Aged from 22 to 42 Days [J]. , 2018, 45(8): 2157-2166.
[9]	YUAN Yingliang, TANG Dan, LU Ying, RAN Guixia. Effects of Dietary Energy and Crude Protein Levels on Growth Performance, Serum Biochemical Indexes and Slaughter Performance of Graylag [J]. , 2018, 45(8): 2227-2235.
[10]	XIE Kan, LI Qingqing, WU Peifu, YANG Yajin, CHEN Fenfen, ZHOU Jielong, GUO Aiwei. Effects of Different Treatments on the Protein Nutritive Value of Jatropha curcas Kernel Meal [J]. , 2018, 45(3): 682-689.
[11]	MA Gong-zhen, LUO Jun, ZHANG Xue-ying, WANG Jian-jue, YANG Yang, SUN Shuang, XI Li-meng. Effects of Concentrate Protein Levels on Growth and Development of Xinong Saanen Dairy Goat Lambs [J]. , 2017, 44(5): 1329-1337.
[12]	CUI Jia-jun, ZHANG He-liang, ZHANG Zhao-qin, LI Ya-kui, LI Guang-dong, ZHAO Xiu-cheng. Effect of Low Crude Protein Diet Supplemented with Amino Acids on Reproductive Performance and Protein Metabolism in Pregnant Sows [J]. , 2016, 43(9): 2310-2316.
[13]	MENG Hong-jiao, ZHU Shi-xin, XIANG Dong, KONG Xian-jie, JIANG Hai-long. Research Progress on Effects of Dietary Crude Protein Levels on Intestinal Barrier Function in Weaned Piglets [J]. , 2016, 43(9): 2496-2501.
[14]	WANG Xian-dong, DENG Hai-feng, LI Hai, JIN Wei-xing, ZHANG Hao, MA Yu-hui, CHEN Yong. Effects of Feeding Different Dietary Crude Protein and Digestible Energy to Yili Mares during Late Lactation Stage on Growth Development and Blood Biochemical Parameters of Foals [J]. , 2015, 42(5): 1137-1144.
[15]	ZHANG Chun, YAN Jia-you, TANG Ling, KUANG Sheng-yao. Effects of Dietary Type and Crude Protein Level on Production Performance and Carcass Traits of Sichuan Mountain Black-bone Chicken [J]. , 2015, 42(10): 2681-2687.