›› 2012, Vol. 39 ›› Issue (12): 205-208.

• 经验交流 • 上一篇    下一篇

寒痢宁口服液的薄层鉴别

王海军, 王胜义, 齐志明, 刘世祥, 荔霞, 刘永明   

  1. 中国农业科学院兰州畜牧与兽药研究所,农业部兽用药物创制重点实验室, 甘肃省中兽药工程技术研究中心,甘肃兰州 730050
  • 收稿日期:2012-05-07 出版日期:2012-12-20 发布日期:2012-12-19
  • 通讯作者: 刘永明(1957-),男,研究员,硕士生导师,主要从事中兽药开发和微量元素代谢病研究。
  • 作者简介:王海军(1985-),男,山东人,硕士生,主要从事中兽药制剂研究与开发。
  • 基金资助:
    中央级公益性科研院所基本科研业务费专项资金项目(BRF110301)。

The TLC Identification of Hanlining Oral Liquid

WANG Hai-jun, WANG Sheng-yi, QI Zhi-ming, LIU Shi-xiang, LI Xia, LIU Yong-ming   

  1. Engineering & Technology Research Center of TCVM of Gansu Province,Key Laboratory of Veterinary Pharmaceutics Discovery,Ministry of Agriculture,Lanzhou Institute of Husbandry and Pharmaceutics Science, Chinese Academy of Agricultural Sciences,Lanzhou 730050,China
  • Received:2012-05-07 Online:2012-12-20 Published:2012-12-19

摘要: 为了建立寒痢宁口服液的质量控制标准,采用薄层色谱法对寒痢宁口服液中的黄连、厚朴、陈皮、补骨脂进行定性鉴定。试验结果表明,黄连、厚朴、陈皮和补骨脂的特征成分在与对照品和对照药材色谱相应位置上显相同颜色的斑点,阴性对照无干扰。该方法专属性强,稳定性和重现性好,为寒痢宁口服液的质量控制建立了定性鉴定方法。

关键词: 寒痢宁口服液; 薄层色谱法; 定性鉴定

Abstract: To establish a quality control standard of Hanlining oral liquid,thin layer chromatography (TLC) was used to qualitatively identify Rhizoma coptidis,Cortex magnoliae offieinalis,Pericarpium citri reticulatae and Fructus psoraleae in preparation. The results showed that the characteristic components of Rhizoma coptidis,Cortex magnoliae offieinalis,Pericarpium citri reticulatae and Fructus psoraleae had same color spots on the same location according to the reference substance and the negative samples had no interference. The TLC identification was highly specific and stable with a good reproducibility, which was a qualitative method for the quality control of Hanlining oral liquid.

Key words: Hanlining oral liquid; TLC; qualitative identification

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